{"id":111,"date":"2018-01-24T08:34:41","date_gmt":"2018-01-24T08:34:41","guid":{"rendered":"http:\/\/www.icmm.csic.es\/realm\/?page_id=111"},"modified":"2018-01-24T08:34:41","modified_gmt":"2018-01-24T08:34:41","slug":"synthesis-techniques","status":"publish","type":"page","link":"https:\/\/wp.icmm.csic.es\/realm\/synthesis-techniques\/","title":{"rendered":"Synthesis techniques"},"content":{"rendered":"

We prepare crystalline nanosized particles by a) hydro\/solvothermal, b) coprecipitation from high boiling point solvents, and\u00a0c) sol-gel and routes.<\/strong> Equipment available at this laboratory includes:<\/p>\n

-Vacuum Schlenk lines.<\/p>\n

-Magnetic stirred hot plates with control of temperature and pH (IKA Ret, IKA C-MAG HS7, with ETS-D5 thermometers).<\/p>\n

-Vortex mixers.<\/p>\n

-50 ml Teflon-lined pressure reactors.<\/p>\n

-Ultrasonic baths.<\/p>\n

-Ultrasonicator device for liquid processing, up 200 W 24 kHZ, with different sonotrodes (Hielscher).<\/p>\n

-Horizontal laminar flow clean cabinet (Aeolus Telstar).<\/p>\n

– Ovens with forced air circulation, up to 300 \u00baC (Memmert UFE500).<\/p>\n

-Centrifuge max 18.000 rpm (Hettich Eba 21).<\/p>\n

-Precision thickness film maker system with heated platens and uniaxial press;<\/p>\n

-Dynamic Light Scattering equipment (Vasco 2, Cordouan Technologies, with NanoQ software) for particle size measurement.<\/p>\n

-Spin-coater with drying system and laminar flow clean bench. Rheometer.<\/p>\n

-Differential Scanning Calorimetry\/ Differential Thermal Analysis (Setaram SetSys Evolution 1700 DTG-DSC, measurements up to 1450 \u00baC).<\/p>\n

-Water distillatory (Water Still Boeco WS 3500).<\/p>\n

-Laboratory refrigerator (Liebherr).<\/p>\n

 <\/p>\n

\"\"<\/p>\n

\"\"<\/p>\n

\"\"<\/p>\n","protected":false},"excerpt":{"rendered":"

We prepare crystalline nanosized particles by a) hydro\/solvothermal, b) coprecipitation from high boiling point solvents, and\u00a0c) sol-gel and routes. Equipment available at this laboratory includes: -Vacuum Schlenk lines. -Magnetic stirred hot plates with control of temperature and pH (IKA Ret, IKA C-MAG HS7, with ETS-D5 thermometers). -Vortex mixers. -50 ml Teflon-lined pressure reactors. -Ultrasonic baths. … <\/p>\n

Continuar leyendo \u00abSynthesis techniques\u00bb<\/span><\/a><\/p>\n","protected":false},"author":51,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-111","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/pages\/111","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/users\/51"}],"replies":[{"embeddable":true,"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/comments?post=111"}],"version-history":[{"count":0,"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/pages\/111\/revisions"}],"wp:attachment":[{"href":"https:\/\/wp.icmm.csic.es\/realm\/wp-json\/wp\/v2\/media?parent=111"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}