- BRUKER NMR Spectometer: AVANCE 400 Console, 9.4 Tesla magnet (400MHz)
- 7 MAS probes to cover different spinning speeds and a wide range of nuclei:
Rotor | MAS spinning speed | Observed frequencies |
2.5 mm | 20 kHz | 31P-15N (162-40.5 MHz)/1H-19F (400-376.5 MHz) |
4 mm | 10 kHz | 31P-15N (162-40.5 MHz)/1H (400MHz) |
4 mm | 10 kHz | 31P-13C (162-100 MHz)/19F (376.5 MHz) |
7 mm | 5 kHz | 31P-13C (162-100 MHz)/1H (400MHz) |
7 mm | 5 kHz | 13C-2H (100-61 MHz)/1H (400MHz) |
7 mm | 5 kHz | 29Si-109Ag (79-18 MHz)/1H (400 MHz) |
- Static probe for pulse field gradient experiments (4 inserts available):
Tube diameter | Observed nucleus | Temperature |
5 mm | 7Li | 300-480 K |
5 mm | 1H | Room temperature |
5 mm | 23Na | 173-473 K |
8 mm | 7Li | Room temperature |
- Static probe for the study of powder and single-crystal for nuclei 31P-109Ag (162-18 MHz).